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The filters are kept frozen until analysis. A quarter of a filter is extracted
by Accelerated Solvent Extraction (ASE) with a mixture of dichloromethane/
hexane (50:50, v/v).
Before extraction, the filters are spiked with deuterium-labelled PAH.
Clean up of the extracts is performed on-line in the extraction cell by adding activated silica.
Analysis of the extracts is carried out by gas chromatography-mass spectrometry
(GC-MS). Concentrations of individual PAH in samples are
corrected for recovery of a deuterium-labelled PAH standard with the
closest molecular weight. A total of 18 PAHs are analyzed in the method.
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